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Pharmaceutical Intermediates

  Acyl Chloride Series

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N-butyryl chloride

        CAS:141-75-3
        Purity:≥98%
        Package:250kg plastic barrel
Chinese Name:Butyryl Chloride         N-butyryl chloride
English Name:Butyryl Chloride        Butanoyl Chloride;
Butyric acid chloride         n-Butyryl chloride
    Molecular formula:C4H7ClO
    Molecular Weight:106.55
    Structure Formula:
               
 Quality Index:      
         Content: ≥98%   
         Boiling point:(Drive off 95%)100℃-104℃     
 Nonvolatile matters:≤0.005%   
 Phosphorous compound:(counted with PO43)%≤0.02%
 Properties:It is with thrilling smell as hydrochloric acid and it is colorless transparent liquid. Freezing point-89℃,Boiling point102℃(100kPa),Relative density1.0277,Refraction rate1.4121. Flashing point<21℃. the product is ether soluble and dissolve on water and alcohol. It is easy to catch on fire with anti-corrosion performance and poisonous smog.  
        Use:It is organic compound intermediates and can be used for the production of butylbenzene and intermediates 2-ethyl-1,3-cyclopentandione.
Preparation method:1.it is the product of butyl acid and thionyl chloride. Heated thionyl chloride to its rebacking and add butyl acid within 4 hours and rebacking for one hour and distill,collecting 95-115℃,and distill for another timeand collect 101-105℃,And the collection rate can be more than 70%. When added phosphors trichloride, the collective rate can be 75%. Industrial products Purity is ≥99%. The proportion of raw materials :Butyric acid890kg/t, thionyl chloride 600kg/t.
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